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Setup List
Holder Status Name ExpNo Experiment User Time Title
25 Completed TO-66-CRUDE 1 N PROTON_SPIN 1H experiment spin on tojanov 00:01:17
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
25 20:40:07 TO-66-CRUDE 1 PROTON_SPIN tojanov + + + + + + +
47 08:14:51 adutta_MS-BAAI 5 AAHMBC sarah - + + - - + + 6.26mg MS-BAAI in 500uL CDCl3
47 07:54:56 adutta_MS-BAAI 4 AAHSQC sarah - + + - - + + 6.26mg MS-BAAI in 500uL CDCl3
47 07:46:32 adutta_MS-BAAI 3 AACOSY sarah - + + - - + + 6.26mg MS-BAAI in 500uL CDCl3
47 07:22:44 adutta_MS-BAAI 2 C13CPD_SIENA sarah - + + - - + + 6.26mg MS-BAAI in 500uL CDCl3
47 07:18:02 adutta_MS-BAAI 1 PROTON_SPIN sarah + + + + + + + 6.26mg MS-BAAI in 500uL CDCl3
46 06:44:36 adutta_MS-TAB 5 AAHMBC sarah - + + - - + + 7.55mg MS-TAB in 500uL CDCl3 +20uL MeOD
46 06:24:39 adutta_MS-TAB 4 AAHSQC sarah - + + - - + + 7.55mg MS-TAB in 500uL CDCl3 +20uL MeOD
46 06:16:17 adutta_MS-TAB 3 AACOSY sarah - + + - - + + 7.55mg MS-TAB in 500uL CDCl3 +20uL MeOD
46 05:52:31 adutta_MS-TAB 2 C13CPD_SIENA sarah - + + - - + + 7.55mg MS-TAB in 500uL CDCl3 +20uL MeOD
46 05:47:46 adutta_MS-TAB 1 PROTON_SPIN sarah + + + + + + + 7.55mg MS-TAB in 500uL CDCl3 +20uL MeOD
45 05:14:20 adutta_MS-MAB 5 AAHMBC sarah - + + - - + + 6.20mg MS-MAB in 500uL CDCl3 +20uL MeOD
45 04:54:24 adutta_MS-MAB 4 AAHSQC sarah - + + - - + + 6.20mg MS-MAB in 500uL CDCl3 +20uL MeOD
45 04:46:01 adutta_MS-MAB 3 AACOSY sarah - + + - - + + 6.20mg MS-MAB in 500uL CDCl3 +20uL MeOD
45 04:22:13 adutta_MS-MAB 2 C13CPD_SIENA sarah - + + - - + + 6.20mg MS-MAB in 500uL CDCl3 +20uL MeOD
45 04:17:30 adutta_MS-MAB 1 PROTON_SPIN sarah + + + + + + + 6.20mg MS-MAB in 500uL CDCl3 +20uL MeOD
44 03:44:04 adutta_MS-MAC 5 AAHMBC sarah - + + - - + + 5.87mg MS-MAC in 500uL CDCl3
44 03:24:08 adutta_MS-MAC 4 AAHSQC sarah - + + - - + + 5.87mg MS-MAC in 500uL CDCl3
44 03:15:48 adutta_MS-MAC 3 AACOSY sarah - + + - - + + 5.87mg MS-MAC in 500uL CDCl3
44 02:52:01 adutta_MS-MAC 2 C13CPD_SIENA sarah - + + - - + + 5.87mg MS-MAC in 500uL CDCl3
44 02:47:30 adutta_MS-MAC 1 PROTON_SPIN sarah + + + + + + + 5.87mg MS-MAC in 500uL CDCl3
43 02:14:04 adutta_MS-GAB 5 AAHMBC sarah - + + - - + + 5.49mg MS-GAB in 500uL CDCl3 +20uL MeOD (not soluble)
43 01:54:08 adutta_MS-GAB 4 AAHSQC sarah - + + - - + + 5.49mg MS-GAB in 500uL CDCl3 +20uL MeOD (not soluble)
43 01:45:45 adutta_MS-GAB 3 AACOSY sarah - + + - - + + 5.49mg MS-GAB in 500uL CDCl3 +20uL MeOD (not soluble)
43 00:59:35 adutta_MS-GAB 2 C13CPD_SIENA sarah - + + - - + + 5.49mg MS-GAB in 500uL CDCl3 +20uL MeOD (not soluble)
43 00:54:52 adutta_MS-GAB 1 PROTON_SPIN sarah + + + + + + + 5.49mg MS-GAB in 500uL CDCl3 +20uL MeOD (not soluble)
42 00:21:27 adutta_MS-AAB 5 AAHMBC sarah - + + - - + + 5.21mg MS-AAB in 500uL CDCl3 +20uL MeOD
42 00:01:31 adutta_MS-AAB 4 AAHSQC sarah - + + - - + + 5.21mg MS-AAB in 500uL CDCl3 +20uL MeOD
42 23:53:10 adutta_MS-AAB 3 AACOSY sarah - + + - - + + 5.21mg MS-AAB in 500uL CDCl3 +20uL MeOD
42 23:29:22 adutta_MS-AAB 2 C13CPD_SIENA sarah - + + - - + + 5.21mg MS-AAB in 500uL CDCl3 +20uL MeOD
42 23:24:22 adutta_MS-AAB 1 PROTON_SPIN sarah + + + + + + + 5.21mg MS-AAB in 500uL CDCl3 +20uL MeOD
41 22:50:56 adutta_MS-AAC 5 AAHMBC sarah - + + - - + + 6.50mg MS-AAC in 500uL CDCl3 +20uL MeOD
41 22:31:00 adutta_MS-AAC 4 AAHSQC sarah - + + - - + + 6.50mg MS-AAC in 500uL CDCl3 +20uL MeOD
41 22:22:37 adutta_MS-AAC 3 AACOSY sarah - + + - - + + 6.50mg MS-AAC in 500uL CDCl3 +20uL MeOD
41 21:58:50 adutta_MS-AAC 2 C13CPD_SIENA sarah - + + - - + + 6.50mg MS-AAC in 500uL CDCl3 +20uL MeOD
41 21:54:00 adutta_MS-AAC 1 PROTON_SPIN sarah + + + + + + + 6.50mg MS-AAC in 500uL CDCl3 +20uL MeOD
40 21:20:34 adutta_MS-PAI 5 AAHMBC sarah - + + - - + + 6.96mg MS-PAI in 500uL CDCl3
40 21:00:39 adutta_MS-PAI 4 AAHSQC sarah - + + - - + + 6.96mg MS-PAI in 500uL CDCl3
40 20:52:18 adutta_MS-PAI 3 AACOSY sarah - + + - - + + 6.96mg MS-PAI in 500uL CDCl3
40 20:28:30 adutta_MS-PAI 2 C13CPD_SIENA sarah - + + - - + + 6.96mg MS-PAI in 500uL CDCl3
40 20:23:43 adutta_MS-PAI 1 PROTON_SPIN sarah + + + + + + + 6.96mg MS-PAI in 500uL CDCl3
39 20:08:40 VF_6_2E 3 C13DEPT135_SIENA vfadare - + + - - + +
39 19:44:52 VF_6_2E 2 C13CPD_SIENA vfadare - + + - - + +
39 19:39:53 VF_6_2E 1 PROTON_SPIN vfadare + + + + + + +
38 19:06:28 adutta_MS-BAAC 5 AAHMBC sarah - + + - - + + 6.72mg MS-BAAC in 500uL CDCl3 + 40uL MeOD (not soluble)
38 18:46:31 adutta_MS-BAAC 4 AAHSQC sarah - + + - - + + 6.72mg MS-BAAC in 500uL CDCl3 + 40uL MeOD (not soluble)
38 18:38:07 adutta_MS-BAAC 3 AACOSY sarah - + + - - + + 6.72mg MS-BAAC in 500uL CDCl3 + 40uL MeOD (not soluble)
38 17:51:54 adutta_MS-BAAC 2 C13CPD_SIENA sarah - + + - - + + 6.72mg MS-BAAC in 500uL CDCl3 + 40uL MeOD (not soluble)
38 17:45:26 adutta_MS-BAAC 1 PROTON_SPIN sarah + + + + + + + 6.72mg MS-BAAC in 500uL CDCl3 + 40uL MeOD (not soluble)
31 17:03:44 JR-1-190 2D 3 AANOESY jrana - + + - - + +
31 16:48:31 JR-1-190 2D 2 AACOSY jrana - + + - - + +
31 16:08:18 JR-1-190 2D 1 AAHSQC jrana + + + + + + +
30 15:33:13 mbg_6_31_f41_47 4 AAHMBC mgarcia - + + - - + +
30 15:13:03 mbg_6_31_f41_47 3 AAHSQC mgarcia - + + - - + +
30 14:49:14 mbg_6_31_f41_47 2 C13CPD_SIENA mgarcia - + + - - + +
30 14:44:18 mbg_6_31_f41_47 1 PROTON_SPIN mgarcia + + + + + + +
29 14:20:27 GM-MG-73-2 2 C13CPD_SIENA gmandal - + + - - + +
29 14:15:48 GM-MG-73-2 1 PROTON_SPIN gmandal + + + + + + +
28 13:51:43 GM-MG-73-1 2 C13CPD_SIENA gmandal - + + - - + +
28 13:46:53 GM-MG-73-1 1 PROTON_SPIN gmandal + + + + + + +
27 13:33:31 PB-2026-255DebenzylationSiena 1 PROTON_SPIN pbonagi + + + + + + +
26 13:09:46 DZ0071098-a 2 C13CPD_SIENA jgalvez - + + - - + +
26 13:04:57 DZ0071098-a 1 PROTON_SPIN jgalvez + + + + + + +
25 12:50:12 DZ0071091B 3 AACOSY jgalvez - + + - - + +
25 12:26:24 DZ0071091B 2 C13CPD_SIENA jgalvez - + + - - + +
25 12:21:59 DZ0071091B 1 PROTON_SPIN jgalvez + + + + + + +
24 12:13:37 DZ0071091A 3 AACOSY jgalvez - + + - - + +
24 11:49:47 DZ0071091A 2 C13CPD_SIENA jgalvez - + + - - + +
24 11:45:12 DZ0071091A 1 PROTON_SPIN jgalvez + + + + + + +
23 11:39:24 DZ0071093-F31 1 PROTON_SPIN jgalvez + + + + + + +
22 11:34:48 DZ0071093-F27 1 PROTON_SPIN jgalvez + + + + + + +
21 11:21:28 DZ-0050-111-A-13C 1 C13CPD_SIENA tzehnder + + + + + + +
20 11:18:23 DZ-0050-111-A-1H 1 PROTON_SPIN tzehnder - + + - - + +
20 11:09:03 DZ-0050-111-A-1H 2 AACOSY tzehnder - + + - - + +
20 11:04:11 DZ-0050-111-A-1H 3 F19 tzehnder + + + + + + + sref: NUCLEUS '19F' not defined for SOLVENT 'DMSO' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'DMSO' SR is set to 0.0
19 10:59:57 DZ-0070-133-C-C18 4 F19 tzehnder - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'MeOD' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'MeOD' SR is set to 0.0
19 10:51:37 DZ-0070-133-C-C18 3 AACOSY tzehnder - + + - - + +
19 10:31:25 DZ-0070-133-C-C18 2 C13CPD_SIENA tzehnder - + + - - + +
19 10:27:03 DZ-0070-133-C-C18 1 PROTON_SPIN tzehnder + + + + + + +
18 10:24:43 DZ-0070-133-B-C18 1 PROTON_SPIN tzehnder - + + - - + +
18 10:15:26 DZ-0070-133-B-C18 3 AACOSY tzehnder - + + - - + +
18 09:54:24 DZ-0070-133-B-C18 2 C13CPD_SIENA tzehnder - + + - - + +
18 09:50:19 DZ-0070-133-B-C18 4 F19 tzehnder + + + + + + + sref: NUCLEUS '19F' not defined for SOLVENT 'MeOD' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'MeOD' SR is set to 0.0
17 09:45:51 DZ-0070-133-A-C18 4 F19 tzehnder - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'MeOD' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'MeOD' SR is set to 0.0
17 09:37:28 DZ-0070-133-A-C18 3 AACOSY tzehnder - + + - - + +
17 09:17:19 DZ-0070-133-A-C18 2 C13CPD_SIENA tzehnder - + + - - + +
17 09:11:53 DZ-0070-133-A-C18 1 PROTON_SPIN tzehnder + + + + + + +
34 06:18:54 adutta_MS-PAB 5 AAHMBC sarah - + + - - + + 5.16mg MS-PAB in 500uL CDCl3
34 05:59:00 adutta_MS-PAB 4 AAHSQC sarah - + + - - + + 5.16mg MS-PAB in 500uL CDCl3
34 05:50:40 adutta_MS-PAB 3 AACOSY sarah - + + - - + + 5.16mg MS-PAB in 500uL CDCl3
34 05:26:54 adutta_MS-PAB 2 C13CPD_SIENA sarah - + + - - + + 5.16mg MS-PAB in 500uL CDCl3
34 05:22:08 adutta_MS-PAB 1 PROTON_SPIN sarah + + + + + + + 5.16mg MS-PAB in 500uL CDCl3
33 04:48:43 adutta_MS-PAC 5 AAHMBC sarah - + + - - + + 8.94mg MS-PAC in 500uL CDCl3
33 04:28:49 adutta_MS-PAC 4 AAHSQC sarah - + + - - + + 8.94mg MS-PAC in 500uL CDCl3
33 04:20:27 adutta_MS-PAC 3 AACOSY sarah - + + - - + + 8.94mg MS-PAC in 500uL CDCl3
33 03:56:40 adutta_MS-PAC 2 C13CPD_SIENA sarah - + + - - + + 8.94mg MS-PAC in 500uL CDCl3
33 03:51:48 adutta_MS-PAC 1 PROTON_SPIN sarah + + + + + + + 8.94mg MS-PAC in 500uL CDCl3
32 03:18:22 adutta_MS-PhGA 5 AAHMBC sarah - + + - - + + 5.36mg MS-PhGA in 500uL CDCl3 + 20uL MeOD
32 02:58:28 adutta_MS-PhGA 4 AAHSQC sarah - + + - - + + 5.36mg MS-PhGA in 500uL CDCl3 + 20uL MeOD
32 02:50:05 adutta_MS-PhGA 3 AACOSY sarah - + + - - + + 5.36mg MS-PhGA in 500uL CDCl3 + 20uL MeOD
32 02:26:15 adutta_MS-PhGA 2 C13CPD_SIENA sarah - + + - - + + 5.36mg MS-PhGA in 500uL CDCl3 + 20uL MeOD
32 02:21:17 adutta_MS-PhGA 1 PROTON_SPIN sarah + + + + + + + 5.36mg MS-PhGA in 500uL CDCl3 + 20uL MeOD
31 01:47:51 adutta_MS-PhA 5 AAHMBC sarah - + + - - + + 5.52mg MS-PhA in 500uL CDCl3 + 20uL MeOD
31 01:27:55 adutta_MS-PhA 4 AAHSQC sarah - + + - - + + 5.52mg MS-PhA in 500uL CDCl3 + 20uL MeOD
31 01:19:33 adutta_MS-PhA 3 AACOSY sarah - + + - - + + 5.52mg MS-PhA in 500uL CDCl3 + 20uL MeOD
31 00:55:45 adutta_MS-PhA 2 C13CPD_SIENA sarah - + + - - + + 5.52mg MS-PhA in 500uL CDCl3 + 20uL MeOD
31 00:51:16 adutta_MS-PhA 1 PROTON_SPIN sarah + + + + + + + 5.52mg MS-PhA in 500uL CDCl3 + 20uL MeOD
30 00:17:51 SR-121-PURE 7 AAHMBC srang - + + - - + +
30 23:40:15 SR-121-PURE 6 AAHSQC_COUP_F2 srang - + + - - + +
30 23:20:19 SR-121-PURE 5 AAHSQC srang - + + - - + +
30 23:11:59 SR-121-PURE 4 AACOSY srang - + + - - + +
30 22:57:00 SR-121-PURE 3 C13DEPT135_SIENA srang - + + - - + +
30 22:33:14 SR-121-PURE 2 C13CPD_SIENA srang - + + - - + +
30 22:28:22 SR-121-PURE 1 PROTON_SPIN srang + + + + + + +
29 22:08:26 VF_7_12_F35_39 5 AAHSQC vfadare - + + - - + +
29 22:00:04 VF_7_12_F35_39 4 AACOSY vfadare - + + - - + +
29 21:45:04 VF_7_12_F35_39 3 C13DEPT135_SIENA vfadare - + + - - + +
29 21:21:14 VF_7_12_F35_39 2 C13CPD_SIENA vfadare - + + - - + +
29 21:16:04 VF_7_12_F35_39 1 PROTON_SPIN vfadare + + + + + + +
28 20:42:39 adutta_MS-APA 5 AAHMBC sarah - + + - - + + 5.18mg MS-APA in 500uL CDCl3 + 20uL MeOD
28 20:22:43 adutta_MS-APA 4 AAHSQC sarah - + + - - + + 5.18mg MS-APA in 500uL CDCl3 + 20uL MeOD
28 20:14:19 adutta_MS-APA 3 AACOSY sarah - + + - - + + 5.18mg MS-APA in 500uL CDCl3 + 20uL MeOD
28 19:28:06 adutta_MS-APA 2 C13CPD_SIENA sarah - + + - - + + 5.18mg MS-APA in 500uL CDCl3 + 20uL MeOD
28 19:22:24 adutta_MS-APA 1 PROTON_SPIN sarah + + + + + + + 5.18mg MS-APA in 500uL CDCl3 + 20uL MeOD
15 18:48:35 adutta_MS-ABA 5 AAHMBC sarah - + + - - + + 5.14mg MS-ABA in 500uL CDCl3 + 20uL MeOD
15 18:28:39 adutta_MS-ABA 4 AAHSQC sarah - + + - - + + 5.14mg MS-ABA in 500uL CDCl3 + 20uL MeOD
15 18:20:16 adutta_MS-ABA 3 AACOSY sarah - + + - - + + 5.14mg MS-ABA in 500uL CDCl3 + 20uL MeOD
15 17:34:08 adutta_MS-ABA 2 C13CPD_SIENA sarah - + + - - + + 5.14mg MS-ABA in 500uL CDCl3 + 20uL MeOD
15 17:29:34 adutta_MS-ABA 1 PROTON_SPIN sarah + + + + + + + 5.14mg MS-ABA in 500uL CDCl3 + 20uL MeOD
14 16:55:43 adutta_MS-BAA 5 AAHMBC sarah - + + - - + + 4.51mg MS-BAA in 500uL CDCl3 + 20uL MeOD
14 16:35:43 adutta_MS-BAA 4 AAHSQC sarah - + + - - + + 4.51mg MS-BAA in 500uL CDCl3 + 20uL MeOD
14 16:27:20 adutta_MS-BAA 3 AACOSY sarah - + + - - + + 4.51mg MS-BAA in 500uL CDCl3 + 20uL MeOD
14 16:03:31 adutta_MS-BAA 2 C13CPD_SIENA sarah - + + - - + + 4.51mg MS-BAA in 500uL CDCl3 + 20uL MeOD
14 15:58:33 adutta_MS-BAA 1 PROTON_SPIN sarah + + + + + + + 4.51mg MS-BAA in 500uL CDCl3 + 20uL MeOD
13 15:25:07 adutta_MS-TA 5 AAHMBC sarah - + + - - + + 6.55mg MS-TA in 500uL CDCl3 + 20uL MeOD
13 15:05:10 adutta_MS-TA 4 AAHSQC sarah - + + - - + + 6.55mg MS-TA in 500uL CDCl3 + 20uL MeOD
13 14:56:47 adutta_MS-TA 3 AACOSY sarah - + + - - + + 6.55mg MS-TA in 500uL CDCl3 + 20uL MeOD
13 14:32:26 adutta_MS-TA 2 C13CPD_SIENA sarah - + + - - + + 6.55mg MS-TA in 500uL CDCl3 + 20uL MeOD
13 14:26:44 adutta_MS-TA 1 PROTON_SPIN sarah + + + + + + + 6.55mg MS-TA in 500uL CDCl3 + 20uL MeOD
12 14:02:55 JAM-2-237 2 C13CPD_SIENA jmand - + + - - + +
12 13:58:07 JAM-2-237 1 PROTON_SPIN jmand + + + + + + +
11 13:50:04 PB-2026-254DebenzylationSiena 1 PROTON_SPIN pbonagi + + + + + + +
10 13:42:04 PB-2026-252DebenzylationSecondPurifiedSiena 1 PROTON_SPIN pbonagi + + + + + + +
9 13:08:38 adutta_MS-AA 5 AAHMBC sarah - + + - - + + 4.79mg MS-AA in 500uL CDCl3 + 20uL MeOD
9 12:46:29 adutta_MS-AA 4 AAHSQC sarah - + + - - + + 4.79mg MS-AA in 500uL CDCl3 + 20uL MeOD
9 12:35:27 adutta_MS-AA 3 AACOSY sarah + + + + + + + 4.79mg MS-AA in 500uL CDCl3 + 20uL MeOD
8 12:32:56 JR-1-190 Qmac PA D2O 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
8 12:27:41 JR-1-190 Qmac PA D2O 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
8 12:22:47 JR-1-190 Qmac PA D2O 1 PROTON_SPIN jrana + + + + + + +
7 11:58:58 adutta_MS-AA 2 C13CPD_SIENA sarah - + + - - + + 4.79mg MS-AA in 500uL CDCl3 + 20uL MeOD
7 11:53:41 adutta_MS-AA 1 PROTON_SPIN sarah + + + + + + + 4.79mg MS-AA in 500uL CDCl3 + 20uL MeOD
4 11:49:02 JR-1-190 Qmac 1 PROTON_SPIN jrana + + + + + + +
3 11:15:36 adutta_MS-PA 5 AAHMBC sarah - + + - - + + 6.38mg MS-PA in 500uL CDCl3
3 10:55:39 adutta_MS-PA 4 AAHSQC sarah - + + - - + + 6.38mg MS-PA in 500uL CDCl3
3 10:47:15 adutta_MS-PA 3 AACOSY sarah - + + - - + + 6.38mg MS-PA in 500uL CDCl3
3 10:21:19 adutta_MS-PA 2 C13CPD_SIENA sarah - + + - - + + 6.38mg MS-PA in 500uL CDCl3
3 10:16:20 adutta_MS-PA 1 PROTON_SPIN sarah + + + + + + + 6.38mg MS-PA in 500uL CDCl3
2 20:47:03 to-Ca-F 3 F19CPD tojanov - + + - - + + sref: reference peak outside file limits default calibration done, sref: reference peak outside file limits default calibration done
2 20:41:55 to-Ca 1 PROTON_SPIN tojanov + + + + + + +
1 20:35:49 to-K-F 4 F19CPD tojanov - + + - - + + sref: reference peak outside file limits default calibration done, sref: reference peak outside file limits default calibration done
1 20:31:04 to-K 5 PROTON_SPIN tojanov + + + + + + +
22 19:07:15 mk-2-110 2 C13CPD_SIENA mkothari - + + - - + +
22 19:02:15 mk-2-110 1 PROTON_SPIN mkothari + + + + + + +
21 18:58:29 JR-1-190 pH 12.51 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
21 18:56:06 JR-1-190 pH 12.51 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
21 18:51:53 JR-1-190 pH 12.51 1 PROTON_SPIN jrana + + + + + + +
20 18:44:28 JR-1-190 pH 11.50 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
20 18:42:19 JR-1-190 pH 11.50 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
20 18:38:04 JR-1-190 pH 11.50 1 PROTON_SPIN jrana + + + + + + +
19 18:31:57 JR-1-190 pH 10.45 3 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
19 18:29:30 JR-1-190 pH 10.45 2 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
19 18:25:02 JR-1-190 pH 10.45 1 PROTON_SPIN jrana + + + + + + +
18 18:14:03 JR-1-190 pH 9.78 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
18 18:11:48 JR-1-190 pH 9.78 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
18 18:07:27 JR-1-190 pH 9.78 1 PROTON_SPIN jrana + + + + + + +
18 17:59:47 JR-1-190 pH 9.47 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
18 17:57:32 JR-1-190 pH 9.47 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
18 17:53:11 JR-1-190 pH 9.47 1 PROTON_SPIN jrana + + + + + + +
18 17:44:29 JR-1-190 pH 9.19 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
18 17:42:15 JR-1-190 pH 9.19 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
18 17:37:41 JR-1-190 pH 9.19 1 PROTON_SPIN jrana + + + + + + +
17 17:30:21 JR-1-190 pH 8.95 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
17 17:28:11 JR-1-190 pH 8.95 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
17 17:23:51 JR-1-190 pH 8.95 1 PROTON_SPIN jrana + + + + + + +
17 17:17:14 JR-1-190 pH 8.58 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
17 17:15:02 JR-1-190 pH 8.58 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
17 17:10:40 JR-1-190 pH 8.58 1 PROTON_SPIN jrana + + + + + + +
15 17:02:42 JR-1-190 pH 7.81 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
15 17:00:10 JR-1-190 pH 7.81 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
15 16:54:55 JR-1-190 pH 7.81 1 PROTON_SPIN jrana + + + + + + +
14 16:46:47 PB-2026-253DebenzylationSiena 1 PROTON_SPIN pbonagi + + + + + + +
13 16:44:06 JR-1-190 pH 7.22 3 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
13 16:41:21 JR-1-190 pH 7.22 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'D2O' SR is set to 0.0
13 16:36:14 JR-1-190 pH 7.22 1 PROTON_SPIN jrana + + + + + + +
12 16:33:56 RS-1-007_heated_100min_02112026 2 PROTON_SPIN fgonzal - + + - - + + pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/fgonzal/nmr/RS-1-007_heated_100min_02112026/2/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/fgonzal/nmr/RS-1-007_heated_100min_02112026/2/pdata/1/peaks!
12 16:30:33 RS-1-007_heated_100min_02112026 1 P31CPD fgonzal + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
10 16:19:34 FG-1-182 6 P31CPD fgonzal - + + - - + +
10 16:15:30 FG-1-182 5 PROTON_SPIN fgonzal + + + + + + +
9 16:13:49 FG-1-181 6 PROTON_SPIN fgonzal - + + - - + +
9 16:08:01 FG-1-181 5 P31CPD fgonzal + + + + + + +
8 16:05:08 RS-1-007_heated_100min_02112026 1 PROTON_SPIN fgonzal + + + x - - - Lock failed after multiple attempts, lock: Command 'lock C6D6' failed. Lock is OFF, Command 'lock C6D6' failed. Lock is OFF
5 15:37:03 KG_Negishi_02112026 1 PROTON_SPIN kgour + + + + + + +
2 14:29:57 JR-1-189 Qmac PA MeOH 1 PROTON_SPIN jrana + + + + + + +
1 13:12:16 FG-1-182 4 PROTON_SPIN fgonzal - + + - - + +
1 13:07:26 FG-1-182 3 P31CPD fgonzal + + + + + + +
60 13:03:36 FG-1-181 4 P31CPD fgonzal - + + - - + +
60 12:59:07 FG-1-181 3 PROTON_SPIN fgonzal + + + + + + +
59 19:54:53 mbg_6_26 6 AACOSY mgarcia - + + - - + +
59 19:21:27 mbg_6_26 5 AAHMBC mgarcia - + + - - + +
59 19:01:18 mbg_6_26 4 AAHSQC mgarcia - + + - - + +
59 18:46:14 mbg_6_26 3 C13DEPT135_SIENA mgarcia - + + - - + +
59 18:21:07 mbg_6_26 2 C13CPD_SIENA mgarcia - + + - - + +
59 18:15:49 mbg_6_26 1 PROTON_SPIN mgarcia + + + + + + +
58 18:12:26 FG-1-180 2 P31CPD fgonzal - + + - - + +
58 18:08:49 FG-1-180 1 PROTON_SPIN fgonzal + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/fgonzal/nmr/FG-1-180/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/fgonzal/nmr/FG-1-180/1/pdata/1/peaks!
57 16:47:07 FG-1-182 2 PROTON_SPIN fgonzal - + + - - + +
57 16:42:01 FG-1-182 1 P31CPD fgonzal + + + + + + +
56 16:39:12 FG-1-181 2 P31CPD fgonzal - + + - - + +
56 16:34:35 FG-1-181 1 PROTON_SPIN fgonzal + + + + + + +
55 16:33:00 FG-1-161-Crystals-THF 2 PROTON_SPIN fgonzal - + + - - + + pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/fgonzal/nmr/FG-1-161-Crystals-THF/2/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/fgonzal/nmr/FG-1-161-Crystals-THF/2/pdata/1/peaks!
55 16:28:35 FG-1-161-Crystals-THF 1 P31CPD fgonzal + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
54 16:25:05 FG-1-179-TMEDA 2 P31CPD fgonzal - + + - - + +
54 16:20:26 FG-1-179-TMEDA 1 PROTON_SPIN fgonzal + + + + + + +
53 15:56:36 GM-MG-72-P 2 C13CPD_SIENA gmandal - + + - - + +
53 15:50:27 GM-MG-72-P 1 PROTON_SPIN gmandal + + + + + + +
52 15:21:27 MJ-1-41_and_42 5 AAHSQC mjamshad - + + - - + +
52 15:13:06 MJ-1-41_and_42 4 AACOSY mjamshad - + + - - + +
52 14:58:04 MJ-1-41_and_42 3 C13DEPT135_SIENA mjamshad - + + - - + +
52 14:23:04 MJ-1-41_and_42 2 C13CPD_SIENA mjamshad - + + - - + +
52 14:18:09 MJ-1-41_and_42 1 PROTON_SPIN mjamshad + + + + + + +
51 13:58:04 VF_7_11_F60 4 AAHSQC vfadare - + + - - + +
51 13:43:04 VF_7_11_F60 3 C13DEPT135_SIENA vfadare - + + - - + +
51 13:17:48 VF_7_11_F60 2 C13CPD_SIENA vfadare - + + - - + +
51 13:12:30 VF_7_11_F60 1 PROTON_SPIN vfadare + + + + + + +
50 12:14:54 PB-2026-252DebenzylationSiena 1 PROTON_SPIN pbonagi + + + + + + +
49 11:42:32 FG-1-179 4 P31CPD fgonzal - + + - - + +
49 11:38:19 FG-1-179 3 PROTON_SPIN fgonzal + + + + + + +
60 20:05:47 RA-184-1 2 C13CPD_SIENA raddanki - + + - - + +
60 20:00:01 RA-184-1 1 PROTON_SPIN raddanki + + + + + + +
55 18:17:46 VF_7_10C_F72_75 4 AAHSQC vfadare - + + - - + +
55 18:02:43 VF_7_10C_F72_75 3 C13DEPT135_SIENA vfadare - + + - - + +
55 17:38:58 VF_7_10C_F72_75 2 C13CPD_SIENA vfadare - + + - - + +
55 17:34:07 VF_7_10C_F72_75 1 PROTON_SPIN vfadare + + + + + + +
54 16:24:31 GM-MG-69-crystal-2 2 C13CPD_SIENA gmandal - + + - - + +
54 16:19:34 GM-MG-69-crystal-2 1 PROTON_SPIN gmandal + + + + + + +
52 13:29:03 PB-2026-251DebenzylationSiena 1 PROTON_SPIN pbonagi + + + + + + +
51 12:58:18 to-35-box 1 PROTON_SPIN tojanov + + + + + + +
50 12:33:30 CA-9 21 PROTON_SPIN sksingh + + + + + + + Quantitative 1H temp=67C solvent=DMSO/TFA ns=32 d1=10s
49 12:21:55 CA-8 21 PROTON_SPIN sksingh + + + + + + + Quantitative 1H temp=67C solvent=DMSO/TFA ns=32 d1=10s
48 12:10:18 CA-12 21 PROTON_SPIN sksingh + + + + + + + Quantitative 1H temp=67C solvent=DMSO/TFA ns=32 d1=10s
47 11:58:15 CA-11 21 PROTON_SPIN sksingh + + + + + + + Quantitative 1H temp=67C solvent=DMSO/TFA ns=32 d1=10s
46 11:49:46 CA-10 21 PROTON_SPIN sksingh - - + - - + + Quantitative 1H temp=67C solvent=DMSO/TFA ns=32 d1=10s