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IconNMR Automation Run Status:
Day Experiments: 00:00
Busy Until: Wed 18:59
Night Experiments: 00:00

Setup List
Holder Status Name ExpNo Experiment User Time Title
10 Completed PK-5-35-S4 11 N PROTON_SPIN 1H experiment spin on KanPro 00:01:17 After adding additonal 200 uL CDCl3
34 Completed PK-5-35-S3 2 N C13CPD_SIENA 1D 13C w/1H decoupling KanPro 00:22:30
35 Completed JR-Pyme_mac_F-CO2 2 N C13CPD_SIENA 1D 13C w/1H decoupling jrana 00:45:16
36 Completed MM-01-178M 1 N PROTON_SPIN 1H experiment spin on mmunda 00:02:26
36 Completed MM-01-178M 2 N C13CPD_SIENA 1D 13C w/1H decoupling mmunda 00:44:56
36 Completed MM-01-178M 3 N AACOSY 2D 1H-1H COSY mmunda 00:14:24
36 Completed MM-01-178M 4 N AAHSQC echo/antiecho edited HSQC w/sensitivity improvement w/adiabatic bilevel decoupling w/adiabatic refocussing (w/ gradients in back-INEPT) mmunda 00:36:30
36 Completed MM-01-178M 5 N AAHMBC HMBCGPND mmunda 00:48:15
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
36 18:10:09 MM-01-178M 5 AAHMBC mmunda - + + - - + -
36 17:32:17 MM-01-178M 4 AAHSQC mmunda - + + - - + +
36 17:16:53 MM-01-178M 3 AACOSY mmunda - + + - - + +
36 16:30:38 MM-01-178M 2 C13CPD_SIENA mmunda - + + - - + +
36 16:22:36 MM-01-178M 1 PROTON_SPIN mmunda + + + + + + +
35 11:31:15 JR-Pyme_mac_F-CO2 2 C13CPD_SIENA jrana + + + + + + +
10 11:24:12 PK-5-35-S4 11 PROTON_SPIN KanPro + + + + + + + After adding additonal 200 uL CDCl3
34 11:02:42 PK-5-35-S3 2 C13CPD_SIENA KanPro - + + - - + +
34 10:57:12 PK-5-35-S3 1 PROTON_SPIN KanPro + + + + + + +
32 10:17:51 pkoth-set3 1 PROTON_SPIN pkoth + + + + + + + 1D 1H in CDCl3/DMSO locked on CDCl3 temp=55C ns=32 d1=15 sec
31 10:03:11 pkoth-set2 1 PROTON_SPIN pkoth + + + + + + + 1D 1H in CDCl3/DMSO locked on CDCl3 temp=55C ns=32 d1=15 sec
30 09:52:10 pkoth-set1 1 PROTON_SPIN pkoth - - + - - + + 1D 1H in CDCl3/DMSO locked on CDCl3 temp=55C ns=32 d1=15 sec
29 23:54:59 LMW 2 ligninHSQC sksingh - + + - - + + Automation was stopped by user
29 23:50:23 LMW 1 PROTON_SPIN sksingh + + + + + + +
28 21:25:28 HMW 12 ligninHSQC sksingh - + + - - + +
28 21:20:35 HMW 11 PROTON_SPIN sksingh + + + + + + +
27 18:55:41 AC-8 2 ligninHSQC sksingh - + + - - + +
27 18:50:18 AC-8 1 PROTON_SPIN sksingh + + + + + + +
26 18:26:22 PK-5-35-S4 2 C13CPD_SIENA KanPro - + + - - + +
26 18:21:16 PK-5-35-S4 1 PROTON_SPIN KanPro + + + + + + +
25 18:17:13 PK-5-35-S3 1 PROTON_SPIN KanPro + + + x - - - Lock failed after multiple attempts, lock: Command 'lock CDCl3' failed. Lock is OFF, Command 'lock CDCl3' failed. Lock is OFF
24 17:53:22 PK-5-35-S2 2 C13CPD_SIENA KanPro - + + - - + +
24 17:48:40 PK-5-35-S2 1 PROTON_SPIN KanPro + + + + + + +
23 17:24:50 PK-5-35-S1 2 C13CPD_SIENA KanPro - + + - - + +
23 17:20:03 PK-5-35-S1 1 PROTON_SPIN KanPro + + + + + + +
22 16:53:38 AS-01-229-A 2 C13CPD_SIENA asingh + + + + + + +
21 16:29:50 ng-02-07 2 C13CPD_SIENA nganga - + + - - + +
21 16:23:21 ng-02-07 1 PROTON_SPIN nganga + + + + + + +
20 15:58:57 ng-02-09 2 C13CPD_SIENA nganga + + + + + + +
19 15:10:26 gm-lsm-137-44 2 C13CPD_SIENA gmandal + + + + + + +
18 14:21:55 gm-lsm-137-43 2 C13CPD_SIENA gmandal + + + + + + +
17 13:35:42 gm-lsm-137-42 2 C13CPD_SIENA gmandal - + + - - + +
17 13:29:58 gm-lsm-137-42 1 PROTON_SPIN gmandal + + + + + + +
16 11:52:41 JR-Pyme_mac_F 3 C13DEPT135_SIENA jrana - + + - - + +
16 11:15:02 JR-Pyme_mac_F 2 C13CPD_SIENA jrana + + + + + + +
15 10:08:18 AM-1-146 5 AAHMBC amars - + + - - + +
15 09:48:22 AM-1-146 4 AAHSQC amars - + + - - + +
15 09:40:00 AM-1-146 3 AACOSY amars - + + - - + +
15 09:16:12 AM-1-146 2 C13CPD_SIENA amars - + + - - + +
15 09:11:47 AM-1-146 1 PROTON_SPIN amars + + + + + + +
14 12:31:40 KW-2024-460_Pyrene 3 C13CPD_POLYMER kweka13 - + + - - + +
14 12:25:34 KW-2024-460_Pyrene 2 F19CPD kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
14 12:20:59 KW-2024-460_Pyrene 1 PROTON_SPIN kweka13 + + + + + + +
13 11:39:57 KW-2024-450_tms 3 C13CPD_POLYMER kweka13 - + + - - + +
13 11:36:19 KW-2024-450_tms 2 F19CPD kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'MeOD' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'MeOD' SR is set to 0.0
13 11:31:36 KW-2024-450_tms 1 PROTON_SPIN kweka13 + + + + + + +
11 17:22:01 KW-2024-TMSEtPh_crude 2 F19 kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
11 17:17:23 KW-2024-TMSEtPh_crude 1 PROTON_SPIN kweka13 + + + + + + +
10 23:00:00 AB-01-170-5H 2 C13CPD_SIENA ajiskani + + + + + + +
9 20:30:00 AB-01-168-ACID 2 C13CPD_SIENA ajiskani + + + + + + +
8 19:45:00 AB-01-170-2-5H 2 C13CPD_SIENA ajiskani + + + + + + +
10 19:20:05 AB-01-170-5H 1 PROTON_SPIN ajiskani + + + + + + +
9 19:07:55 AB-01-168-ACID 1 PROTON_SPIN ajiskani + + + + + + +
8 18:47:47 AB-01-170-2-5H 1 PROTON_SPIN ajiskani + + + + + + +
8 18:23:08 AB-01-170-25HH 2 C13CPD_SIENA ajiskani - + + - - + +
8 18:15:21 AB-01-170-25HH 1 PROTON_SPIN ajiskani + + + + + + + lock: Command 'lock CDCl3' failed. Lock is PENDING
8 16:57:56 AB-01-170-25H 2 C13CPD_SIENA ajiskani - + + - - + +
8 16:52:15 AB-01-170-25H 1 PROTON_SPIN ajiskani + + + + x + + topshim: TopshimPerformShimming - too many points lost during fit, Shim failed
7 16:25:48 AB-01-169-C 1 C13CPD_SIENA ajiskani + + + + + + +
6 15:59:31 AB-01-166 1 C13CPD_SIENA ajiskani + + + + + + +
5 15:31:20 AB-01-DF-C 1 C13CPD_SIENA ajiskani + + + + + + +
33 14:21:35 AB-01-170-00 2 C13CPD_SIENA ajiskani - + + - - + +
33 14:16:07 AB-01-170-00 1 PROTON_SPIN ajiskani + + + + + + +
49 23:33:59 JM-2-143-BS1 5 AAHMBC jmartin - + + - - + +
49 23:14:02 JM-2-143-BS1 4 AAHSQC jmartin - + + - - + +
49 23:05:36 JM-2-143-BS1 3 AACOSY jmartin - + + - - + +
49 22:41:23 JM-2-143-BS1 2 C13CPD_SIENA jmartin - + + - - + +
49 22:35:52 JM-2-143-BS1 1 PROTON_SPIN jmartin + + + + + + +
1 22:07:02 DZ-00497-149_f16-28_13C 4 C13DEPT135_SIENA tzehnder - + + - - + +
1 21:38:21 DZ-00497-149_f16-28_13C 3 C13DEPT90 tzehnder - + + - - + +
1 21:06:03 DZ-00497-149_f16-28_13C 2 C13CPD_SIENA tzehnder + + + + + + +
60 20:57:40 DZ-00497-149_f16-28_1H 2 AACOSY tzehnder - + + - - + +
60 20:48:11 DZ-00497-149_f16-28_1H 1 PROTON_SPIN tzehnder + + + + + + +
59 20:19:34 DZ-00497-149_f14-15_13C 4 C13DEPT135_SIENA tzehnder - + + - - + +
59 19:50:46 DZ-00497-149_f14-15_13C 3 C13DEPT90 tzehnder - + + - - + +
59 19:17:54 DZ-00497-149_f14-15_13C 2 C13CPD_SIENA tzehnder + + + + + + +
58 19:09:06 DZ-00497-149_f14-15_1H 2 AACOSY tzehnder - + + - - + +
58 18:57:01 DZ-00497-149_f14-15_1H 1 PROTON_SPIN tzehnder + + + + + + +
57 18:48:41 DZ-0049-027B_f27-50_f27-37 5 AACOSY tzehnder - + + - - + +
57 17:53:22 DZ-0049-027B_f27-50_f27-37 4 C13DEPT135_SIENA tzehnder - + + - - + +
57 16:57:54 DZ-0049-027B_f27-50_f27-37 3 C13DEPT90 tzehnder - + + - - + +
57 16:02:22 DZ-0049-027B_f27-50_f27-37 2 C13CPD_SIENA tzehnder - + + - - + +
57 15:52:40 DZ-0049-027B_f27-50_f27-37 1 PROTON_SPIN tzehnder + + + + + + +
56 10:30:39 RG-2024-189-polymer-30mg 1 PROTON_SPIN rgorla + + + + + + +
53 10:09:00 RG-2024-188-polymer-100mg 1 PROTON_SPIN rgorla + + + + + + +
53 18:29:06 JM-2-141 5 AAHMBC jmartin - + + - - + +
53 18:09:10 JM-2-141 4 AAHSQC jmartin - + + - - + +
53 18:00:25 JM-2-141 3 AACOSY jmartin - + + - - + +
53 17:14:05 JM-2-141 2 C13CPD_SIENA jmartin - + + - - + +
53 17:05:11 JM-2-141 1 PROTON_SPIN jmartin + + + + + + +
52 12:23:37 DZ-0049-033-B-1H 1 PROTON_SPIN tzehnder - + + + + + + 1D 1H in D2O/DCl temp=70C ns=64 d1=8 Sec TD (size of FID)=32768 sw=20 ppm (10000 Hz) lb=1 equiilibrated at 70C for 10 min before scanning
51 11:44:14 DZ-0049-033-A-1H 1 PROTON_SPIN tzehnder - + + + + + + 1D 1H in D2O/DCl temp=70C ns=64 d1=8 Sec TD (size of FID)=32768 sw=20 ppm (10000 Hz) lb=1 equiilibrated at 70C for 10 min before scanning Automation was stopped by user
50 19:47:52 SLM-02-50P 1 C13CPD_SIENA smali + + + + + + + Automation was stopped by user
49 19:21:25 SLM-02-50-B1 1 C13CPD_SIENA smali + + + + + + +
48 19:16:14 ng-02-06 1 PROTON_SPIN nganga + + + + + + +
47 19:01:13 mgb_5_0_ac_15h 3 C13DEPT135_SIENA mgarcia - + + - - + +
47 18:36:09 mgb_5_0_ac_15h 2 C13CPD_SIENA mgarcia - + + - - + +
47 18:31:06 mgb_5_0_ac_15h 1 PROTON_SPIN mgarcia + + + + + + +
46 13:32:37 KW-2024-446 2 F19CPD kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
46 13:27:52 KW-2024-446 1 PROTON_SPIN kweka13 + + + + + + +
45 13:24:49 KW-2024-445 2 F19CPD kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
45 13:20:15 KW-2024-445 1 PROTON_SPIN kweka13 + + + + + + +
44 13:16:35 KW-2024-444 2 F19CPD kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
44 13:11:51 KW-2024-444 1 PROTON_SPIN kweka13 + + + + + + +
43 13:08:47 KW-2024-443 2 F19CPD kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
43 13:04:12 KW-2024-443 1 PROTON_SPIN kweka13 + + + + + + +
42 13:00:59 KW-2024-442 2 F19CPD kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
42 12:56:25 KW-2024-442 1 PROTON_SPIN kweka13 + + + + + + +
41 12:50:31 KW-2024-441 2 F19CPD kweka13 - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'CDCl3' SR is set to 0.0
41 12:45:32 KW-2024-441 1 PROTON_SPIN kweka13 + + + + + + +
25 10:32:32 AM-1-134 5 AAHMBC amars - + + - - + +
25 10:12:36 AM-1-134 4 AAHSQC amars - + + - - + +
25 10:04:11 AM-1-134 3 AACOSY amars - + + - - + +
25 09:40:22 AM-1-134 2 C13CPD_SIENA amars - + + - - + +
25 09:35:45 AM-1-134 1 PROTON_SPIN amars + + + + + + +
48 16:10:05 RG-2024-183-polymer-100mg 2 PROTON_SPIN rgorla + + + + + + +
46 15:57:07 RG-2024-187-polymer-100mg 1 PROTON_SPIN rgorla + + + + + + +
45 15:29:47 JR-1-91 2 C13CPD_SIENA jrana + + + + + + +
44 14:00:47 cp-2-117 2 F19CPD cparan - + + - - + + sref: reference peak outside file limits default calibration done, sref: reference peak outside file limits default calibration done
44 13:55:26 cp-2-117 1 PROTON_SPIN cparan + + + + + + +
29 11:49:22 RG-2024-186-polymer-100mg 1 PROTON_SPIN rgorla + + + + + + +
26 11:36:31 RG-2024-185-polymer-100mg 1 PROTON_SPIN rgorla + + + + + + +
23 11:23:36 RG-2024-184-polymer-100mg 1 PROTON_SPIN rgorla + + + + + + +
20 11:04:38 RG-2024-183-polymer-100mg 1 PROTON_SPIN rgorla + + + + + + +
18 19:28:50 RG-2-L5UO2-20241111 1 PROTON_SPIN garehar + + + + + + +
11 16:05:38 pkoth-2 1 PROTON_SPIN pkoth + + + + + + + 1D 1H in CDCl3 temp=55C ns=32 d1=15 sec
10 15:51:04 pkoth-1-A 1 PROTON_SPIN pkoth + + + + + + + 1D 1H in CDCl3 temp=55C ns=32 d1=15 sec
9 15:39:29 pkoth-1-I 1 PROTON_SPIN pkoth - - + - - + + 1D 1H in CDCl3 temp=55C ns=32 d1=15 sec
15:21:44 Start-Up - - - - - - - Automation was stopped by user