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Day Experiments: 02:23
Busy Until: Thu 19:52
Night Experiments: 00:00

Setup List
Holder Status Name ExpNo Experiment User Time Title
1 Submitted A004-6A 2 N ligninHSQC 2D 1H-13C HSQC (non-edited); 1td 256; 1sw 210ppm; ns 16 nmark 02:23:26
11 Completed A004-6A 1 N PROTON_SPIN 1H experiment spin on nmark 00:14:26 Quantitative 1H sample=A004-6A solvent=DMSO pulprog=zg ns=16 ds=4 p1=11.7us d1=40sec
12 Completed dakhavan_Gln-white_260326 1 N PROTON_SPIN 1H experiment spin on raulns 00:01:17
13 Completed dakhavan_Gln-black_260326 1 N PROTON_SPIN 1H experiment spin on raulns 00:01:17
13 Completed dakhavan_Gln-black_260326 2 N PROTON_SPIN 1H experiment spin on raulns 00:04:44 1D 1H 3.1mg Gln-black in 600 uL DMSO ns=64
14 Completed dakhavan_Gln-washing_260326 1 N PROTON_SPIN 1H experiment spin on raulns 00:04:44 1D 1H 10mg Gln-washing in 600uL DMSO ns=64
15 Completed O3MIX 1 N PROTON_SPIN 1H experiment spin on nmark 00:14:26 Quantitative 1H sample=O3MIX solvent=DMSO pulprog=zg ns=16 ds=4 p1=11.7us d1=40sec
16 Completed A004-6B 1 N PROTON_SPIN 1H experiment spin on nmark 00:14:26 Quantitative 1H sample=A004-6B solvent=DMSO pulprog=zg ns=16 ds=4 p1=11.7us d1=40sec
17 Completed RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026 3 N PROTON_SPIN 1H experiment spin on rshippy 00:01:17
17 Completed RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026 4 N P31CPD 31P exp. comp. pulse decoupling rshippy 00:00:49
17 Completed RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026 5 N PROTON_SPIN_NoD_shim rshippy 00:01:17
18 Completed RS-1-038_Al2H2bisphos_Ni(COD)2_crude_solution_pentane_03262026 1 N PROTON_SPIN_NoD_shim rshippy 00:01:17
18 Completed RS-1-038_Al2H2bisphos_Ni(COD)2_crude_solution_pentane_03262026 2 N P31CPD 31P exp. comp. pulse decoupling rshippy 00:00:49
37 Completed dakhavan_Gln-white_260326 2 N PROTON_SPIN 1H experiment spin on raulns 00:04:44 1D 1H 7.5mg Gln-white in 600uL DMSO ns=64
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
18 17:25:40 RS-1-038_Al2H2bisphos_Ni(COD)2_crude_solution_pentane_03262026 2 P31CPD rshippy - + + - - + -
18 17:19:12 RS-1-038_Al2H2bisphos_Ni(COD)2_crude_solution_pentane_03262026 1 PROTON_SPIN_NoD_shim rshippy + + + + - + + hwcal: Width at half height : 81.59 Hz, Width at half height : 81.59 Hz, Width at half height : 81.59 Hz, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-038_Al2H2bisphos_Ni(COD)2_crude_solution_pentane_03262026/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-038_Al2H2bisphos_Ni(COD)2_crude_solution_pentane_03262026/1/pdata/1/peaks!
17 17:15:28 RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026 5 PROTON_SPIN_NoD_shim rshippy - + + - - + + hwcal: Width at half height : 16.99 Hz, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026/5/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026/5/pdata/1/peaks!
17 17:11:35 RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026 4 P31CPD rshippy - + + - - + + pp: Cannot find any peak for scaling in /opt/topspin/data/rshippy/nmr/RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026/4/pdata/1/peaks!, pp: Cannot find any peak for scaling in /opt/topspin/data/rshippy/nmr/RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026/4/pdata/1/peaks!
17 17:08:07 RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026 3 PROTON_SPIN rshippy + + + + - + + pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026/3/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-039_Al2H2bisphos+Ni(COD)_crude_solid_pentane_03262026/3/pdata/1/peaks!
16 16:04:08 A004-6B 1 PROTON_SPIN nmark + + + + + + + Quantitative 1H sample=A004-6B solvent=DMSO pulprog=zg ns=16 ds=4 p1=11.7us d1=40sec
15 15:44:10 O3MIX 1 PROTON_SPIN nmark + + + + + + + Quantitative 1H sample=O3MIX solvent=DMSO pulprog=zg ns=16 ds=4 p1=11.7us d1=40sec
14 15:35:05 dakhavan_Gln-washing_260326 1 PROTON_SPIN raulns + + + + + + + 1D 1H 10mg Gln-washing in 600uL DMSO ns=64
37 15:25:57 dakhavan_Gln-white_260326 2 PROTON_SPIN raulns + + + + + + + 1D 1H 7.5mg Gln-white in 600uL DMSO ns=64
13 15:20:04 dakhavan_Gln-black_260326 2 PROTON_SPIN raulns - + + - - + + 1D 1H 3.1mg Gln-black in 600 uL DMSO ns=64
13 15:11:17 dakhavan_Gln-black_260326 1 PROTON_SPIN raulns + + + + + + +
12 15:06:44 dakhavan_Gln-white_260326 1 PROTON_SPIN raulns + + + + + + +
11 14:47:55 A004-6A 1 PROTON_SPIN nmark - - + - - + + Quantitative 1H sample=A004-6A solvent=DMSO pulprog=zg ns=16 ds=4 p1=11.7us d1=40sec
9 12:47:57 FG-ReducePyVTSample 1 DEUTERIUM fgonzal + + + + - x - lock: lock +afterholdon: No sucess, Acquisition Failed, Automation was stopped by user
7 11:05:45 NiMg-2FPy 8 C13CPD_SIENA fgonzal + + + + + + +
7 10:54:16 NiMg-2FPy 7 PROP31DEC fgonzal + + + + + + +
5 10:51:12 RS-1-038_Al2H2bisphos+Ni(COD)2_crude_ether_03262026 2 P31CPD rshippy - + + - - + +
5 10:47:34 RS-1-038_Al2H2bisphos+Ni(COD)2_crude_ether_03262026 1 PROTON_SPIN rshippy + + + + - + + pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-038_Al2H2bisphos+Ni(COD)2_crude_ether_03262026/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-038_Al2H2bisphos+Ni(COD)2_crude_ether_03262026/1/pdata/1/peaks!
3 09:50:34 JG-02-008-et2o 2 PROTON_SPIN jgipper - + + - - + +
3 09:45:58 JG-02-008-et2o 1 P31CPD jgipper + + + + + + +
2 09:42:47 JG-02-008-pen 2 P31CPD jgipper - + + - - + +
2 09:37:45 JG-02-008-pen 1 PROTON_SPIN jgipper + + + + + + +
1 09:05:36 FG-1-198 12 P31CPD fgonzal - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0
1 09:01:49 FG-1-198 11 PROTON_SPIN fgonzal + + + + + + +
24 18:42:33 FG-1-195 4 PROTON_SPIN fgonzal - + + - - + +
24 18:37:10 FG-1-195 3 P31CPD fgonzal + + + + + + +
23 18:35:00 FG-1-198 10 P31CPD fgonzal - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0
23 18:30:32 FG-1-198 9 PROTON_SPIN fgonzal + + + + + + +
22 17:57:25 GAR-1-016 1 PROTON_SPIN grout + + + + + + +
21 16:10:39 IA-CR-301_16 2 PROTON_SPIN raulns + + + + + + + 1D 1H 7.3 mg IA-CR-301-16 om 600 uL DMSO
20 16:04:40 IA-CR-301_15 1 PROTON_SPIN raulns + + + + + + + 1D 1H 6.0 mg IA-CR-301-15 om 600 uL DMSO
19 15:58:47 IA-CR-301_14 1 PROTON_SPIN raulns + + + + + + + 1D 1H 5.4 mg IA-CR-301-14 om 600 uL DMSO
18 15:52:36 IA-CR-301_13 1 PROTON_SPIN raulns + + + + + + + 1D 1H 5.7 mg IA-CR-301-13 om 600 uL DMSO
17 15:33:29 FG-1-198 8 PROTON_SPIN fgonzal - + + - - + +
17 15:28:10 FG-1-198 7 P31CPD fgonzal + + + + + + + sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0
17 15:26:13 FG-1-196 3 P31CPD fgonzal x - - - - - - Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 17
16 15:24:00 FG-1-198 6 P31CPD fgonzal - + + - - + +
16 15:19:15 FG-1-198 5 PROTON_SPIN fgonzal + + + + + + +
12 14:59:01 JG-DD-01-002-L-Al-Et 4 AACOSY jgipper - + + - - + +
12 14:55:13 JG-DD-01-002-L-Al-Et 3 P31CPD jgipper - + + - - + +
12 14:52:54 JG-DD-01-002-L-Al-Et 2 PROTON_SPIN jgipper - + + - - + +
12 14:48:29 JG-DD-01-002-L-Al-Et 1 PROTON_SPIN jgipper + + + + + + +
10 14:10:25 IA-CR-301_16 1 PROTON_SPIN raulns + + + + + + + 1D 1H 7.3 mg IA-R-301-16 om 600 uL DMSO
9 13:54:51 FG-1-198 4 P31CPD fgonzal - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0
9 13:50:23 FG-1-198 3 PROTON_SPIN fgonzal + + + + + + +
8 13:26:45 KJ-2026-P-OMe 3 AAHSQC kjacob + + + + + + +
7 12:35:31 FG-1-198 2 P31CPD fgonzal - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'Pyr' SR is set to 0.0
7 12:30:48 FG-1-198 1 PROTON_SPIN fgonzal + + + + + + +
6 12:10:21 FG-1-197 9 F19CPD fgonzal - + + - - + + sref: reference peak outside file limits default calibration done, sref: reference peak outside file limits default calibration done
6 12:07:12 FG-1-197 8 P31CPD fgonzal - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'Acetone' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'Acetone' SR is set to 0.0
6 12:02:43 FG-1-197 7 PROTON_SPIN fgonzal + + + + + + +
3 10:56:56 JG-02-001-PhH 4 PROTON_SPIN jgipper - + + - - + +
3 10:55:38 JG-02-001-PhH 3 PROTON_SPIN jgipper - + + - - + +
3 10:52:47 JG-02-001-PhH 2 P31CPD jgipper - + + - - + +
3 10:48:16 JG-02-001-PhH 1 PROTON_SPIN jgipper + + + + + + +
2 10:45:49 JG-02-001-ether 2 PROTON_SPIN jgipper - + + - - + +
2 10:40:48 JG-02-001-ether 1 P31CPD jgipper + + + + + + +
1 10:37:06 JG-02-001-pentane 2 P31CPD jgipper - + + - - + +
1 10:31:51 JG-02-001-pentane 1 PROTON_SPIN jgipper + + + + + + +
59 09:58:23 DG-568 58 C13CPD_SIENA dgorve - + + - - + + 1D 13C in CDCl3 temp=57C
59 09:53:20 DG-568 57 PROTON_SPIN dgorve + + + + + + + 1D 1H in CDCl3 temp=57C
58 09:30:29 DG-566 58 C13CPD_SIENA dgorve - + + - - + + 1D 13C in CDCl3 temp=57 C
58 09:27:53 DG-566 57 PROTON_SPIN dgorve - - + - - + + 1D 1H in CDCl3 temp=57 C
57 00:00:03 VF_10524 2 C13CPD_SIENA vfadare - + + - - + + Automation was stopped by user
57 23:54:47 VF_10524 1 PROTON_SPIN vfadare + + + + + + +
56 22:01:09 AK-02-05_Repurified 2 C13CPD_SIENA akaush - + + - - + +
56 21:55:31 AK-02-05_Repurified 1 PROTON_SPIN akaush + + + + + + +
55 21:31:44 VF_7_46 2 C13CPD_SIENA vfadare - + + - - + +
55 21:25:47 VF_7_46 1 PROTON_SPIN vfadare + + + + + + +
54 19:31:51 KJ-2026-P-OMe 2 C13CPD_POLYMER kjacob - + + - - + +
54 19:22:55 KJ-2026-P-OMe 1 PROTON_SPIN kjacob + + + + + + +
50 19:17:31 DZ-0049-0142_try2 1 PROTON_SPIN tzehnder + + + + + + +
49 19:12:04 DZ-0063-046_try2 1 PROTON_SPIN tzehnder + + + + + + +
48 19:07:29 DZ-0063-039_try2 1 PROTON_SPIN tzehnder + + + + + + +
47 18:59:09 DZ-0063-048-E_try2 2 AACOSY tzehnder - + + - - + +
47 18:54:30 DZ-0063-048-E_try2 1 PROTON_SPIN tzehnder + + + + + + +
43 18:46:13 DZ-0063-048-A_try2 2 AACOSY tzehnder - + + - - + +
43 18:41:33 DZ-0063-048-A_try2 1 PROTON_SPIN tzehnder + + + + + + +
42 18:33:18 DZ-0072-009-E 2 AACOSY tzehnder - + + - - + +
42 18:28:18 DZ-0072-009-E 1 PROTON_SPIN tzehnder + + + + + + +
41 18:19:55 DZ-0072-009-D 2 AACOSY tzehnder - + + - - + +
41 18:13:27 DZ-0072-009-D 1 PROTON_SPIN tzehnder + + + + + + +
40 18:10:40 SD-01-034-BEN 2 P31CPD fgonzal - + + - - + + pp: Cannot find any peak for scaling in /opt/topspin/data/fgonzal/nmr/SD-01-034-BEN/2/pdata/1/peaks!, pp: Cannot find any peak for scaling in /opt/topspin/data/fgonzal/nmr/SD-01-034-BEN/2/pdata/1/peaks!
40 18:04:57 SD-01-034-BEN 1 PROTON_SPIN fgonzal + + + + + + +
39 17:59:46 SD-01-034-ETHER 2 P31CPD fgonzal - + + - - + +
39 17:54:13 SD-01-034-ETHER 1 PROTON_SPIN fgonzal + + + + + + +
38 17:51:06 SD-01-034-PEN 2 P31CPD fgonzal - + + - - + +
38 17:46:43 SD-01-034-PEN 1 PROTON_SPIN fgonzal + + + + + + +
37 17:38:26 DZ-0072-009-C 2 AACOSY tzehnder - + + - - + +
37 17:33:39 DZ-0072-009-C 1 PROTON_SPIN tzehnder + + + + + + +
36 17:25:20 DZ-0072-009-B 2 AACOSY tzehnder - + + - - + +
36 17:20:38 DZ-0072-009-B 1 PROTON_SPIN tzehnder + + + + + + +
35 17:12:15 DZ-0072-009-A 2 AACOSY tzehnder - + + - - + +
35 17:06:48 DZ-0072-009-A 1 PROTON_SPIN tzehnder + + + + + + +
34 17:04:22 GAR-1-013-crystal 2 PROTON_SPIN grout - + + - - + +
34 16:59:30 GAR-1-013-crystal 1 P31CPD grout + + + + + + + pp: Cannot find any peak for scaling in /opt/topspin/data/grout/nmr/GAR-1-013-crystal/1/pdata/1/peaks!, pp: Cannot find any peak for scaling in /opt/topspin/data/grout/nmr/GAR-1-013-crystal/1/pdata/1/peaks!
33 16:57:15 GAR-1-012-crystal 2 P31CPD grout - + + - - + + pp: Cannot find any peak for scaling in /opt/topspin/data/grout/nmr/GAR-1-012-crystal/2/pdata/1/peaks!, pp: Cannot find any peak for scaling in /opt/topspin/data/grout/nmr/GAR-1-012-crystal/2/pdata/1/peaks!
33 16:51:32 GAR-1-012-crystal 1 PROTON_SPIN grout + + + + + + +
9 16:48:16 RS-1-037_crude_C6D6_RT24hr_03242026 24 P31CPD rshippy - + + - - + +
9 16:43:26 RS-1-037_crude_C6D6_RT24hr_03242026 23 PROTON_SPIN rshippy + + + + + + +
32 16:41:00 GAR-1-011-crystal 2 PROTON_SPIN grout - + + - - + +
32 16:36:00 GAR-1-011-crystal 1 P31CPD grout + + + + + + +
31 16:33:37 GAR-1-006-crystal 2 P31CPD grout - + + - - + + pp: Cannot find any peak for scaling in /opt/topspin/data/grout/nmr/GAR-1-006-crystal/2/pdata/1/peaks!, pp: Cannot find any peak for scaling in /opt/topspin/data/grout/nmr/GAR-1-006-crystal/2/pdata/1/peaks!
31 16:28:12 GAR-1-006-crystal 1 PROTON_SPIN grout + + + + + + +
30 16:24:10 SD-01-033-ben 2 P31CPD jgipper - + + - - + + pp: Cannot find any peak for scaling in /opt/topspin/data/jgipper/nmr/SD-01-033-ben/2/pdata/1/peaks!, pp: Cannot find any peak for scaling in /opt/topspin/data/jgipper/nmr/SD-01-033-ben/2/pdata/1/peaks!
30 16:19:23 SD-01-033-ben 1 PROTON_SPIN jgipper + + + + + + +
29 16:17:01 SD-01-033-ether 2 PROTON_SPIN jgipper - + + - - + +
29 16:10:43 SD-01-033-ether 1 P31CPD jgipper + + + + + + + pp: Cannot find any peak for scaling in /opt/topspin/data/jgipper/nmr/SD-01-033-ether/1/pdata/1/peaks!, pp: Cannot find any peak for scaling in /opt/topspin/data/jgipper/nmr/SD-01-033-ether/1/pdata/1/peaks!
28 16:04:53 SD-01-033-pen 2 P31CPD jgipper - + + - - + +
28 15:59:38 SD-01-033-pen 1 PROTON_SPIN jgipper + + + + + + +
26 15:56:32 FG-1-197 6 F19CPD fgonzal - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'C6D6' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'C6D6' SR is set to 0.0
26 15:51:21 FG-1-197 5 P31CPD fgonzal - + + - - + +
26 15:46:06 FG-1-197 4 PROTON_SPIN fgonzal + + + + + + +
47 14:04:47 CW-05-152_13C 1 C13CPD_SIENA cwaller + + + + + + +
20 12:45:23 to-92-001 1 PROTON_SPIN tojanov + + + + + + +
18 12:42:29 JG-02-006-1240pm-03-24-2026 2 P31CPD jgipper - + + - - + +
18 12:37:36 JG-02-006-1240pm-03-24-2026 1 PROTON_SPIN jgipper + + + + + + +
16 12:06:33 FG-1-197 3 F19CPD fgonzal + + + + + + + sref: NUCLEUS '19F' not defined for SOLVENT 'C6D6' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'C6D6' SR is set to 0.0
16 11:56:10 FG-1-197 2 P31CPD fgonzal - + + - - + +
16 11:51:14 FG-1-197 1 PROTON_SPIN fgonzal + + + + + + +
15 11:49:01 FG-1-196 2 PROTON_SPIN_NoD_shim fgonzal - + + - - + + hwcal: Width at half height : 26.26 Hz, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/fgonzal/nmr/FG-1-196/2/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/fgonzal/nmr/FG-1-196/2/pdata/1/peaks!
15 11:45:17 FG-1-196 1 P31CPD fgonzal + + + + - + +
14 11:42:10 FG-1-195 2 P31CPD fgonzal - + + - - + +
14 11:38:01 FG-1-195 1 PROTON_SPIN fgonzal + + + + + + +
11 11:03:43 JG-02-008-11am-03-23-2026 2 P31CPD jgipper - + + - - + +
11 11:00:18 JG-02-008-11am-03-23-2026 1 PROTON_SPIN_NoD_shim jgipper + + + + - + + hwcal: Width at half height : 50.25 Hz; topshim: TopshimFieldMap - not enough valid points in centre: the gradient does not work, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/jgipper/nmr/JG-02-008-11am-03-23-2026/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/jgipper/nmr/JG-02-008-11am-03-23-2026/1/pdata/1/peaks!
11 10:56:32 JG-02-008-11am-03-23-2026 1 PROTON_SPIN jgipper + + + x - - - Lock failed after multiple attempts, lock: Command 'lock C6D6' failed. Lock is OFF, Command 'lock C6D6' failed. Lock is OFF
9 09:24:10 RS-1-037_crude_C6D6_RT17hr_03232026 19 PROTON_SPIN rshippy - + + - - + +
9 09:19:45 RS-1-037_crude_C6D6_RT17hr_03232026 18 P31CPD rshippy + + + + + + +
9 02:01:59 RS-1-037_crude_C6D6_RT9hr_03232026 15 P31CPD rshippy - + + - - + +
9 01:55:00 RS-1-037_crude_C6D6_RT9hr_03232026 14 PROTON_SPIN rshippy + + + + + + +
15 00:23:27 new_ascorbyl_palmitate_purity_DMSO_260318 3 PROTON corbion + + + + + + + 1D q1H (redo with longer d1) NEW ascorbyl palmitate - 21.23 mg TCNB - 10.06 mg DMSO - 1 mL pulprog=zg p1=11.5 usec ns=16 d1=220s ds=4 temp=25C user=Sarah date=3/23/26
14 23:01:01 old_ascorbyl_palmitate_purity_DMSO_260318 3 PROTON corbion + + + + + + + 1D q1H (redo with new p1 and d1 values) OLD ascorbyl palmitate - 19.48 mg TCNB - 9.86 mg DMSO - 1 mL pulprog=zg p1=11.8 usec ns=16 d1=220s ds=4 temp=25C user=Sarah date=3/23/26
9 21:59:26 RS-1-037_crude_C6D6_RT5hr_03232026 11 PROTON_SPIN rshippy - + + - - + +
9 21:55:00 RS-1-037_crude_C6D6_RT5hr_03232026 10 P31CPD rshippy + + + + + + +
9 20:57:05 RS-1-037_crude_C6D6_RT3hr_03232026 7 P31CPD rshippy - + + - - + +
9 20:50:35 RS-1-037_crude_C6D6_RT3hr_03232026 6 PROTON rshippy + + + + + + +
11 20:30:39 NiMg-2FPy 6 AAHSQC fgonzal - + + - - + +
11 20:22:14 NiMg-2FPy 5 AACOSY fgonzal - + + - - + +
11 19:55:52 NiMg-2FPy 4 C13CPD_SIENA fgonzal - + + - - + +
11 19:51:30 NiMg-2FPy 3 F19CPD fgonzal - + + - - + + sref: NUCLEUS '19F' not defined for SOLVENT 'C6D6' SR is set to 0.0, sref: NUCLEUS '19F' not defined for SOLVENT 'C6D6' SR is set to 0.0
11 19:47:10 NiMg-2FPy 2 P31CPD fgonzal + + + + + + +
11 19:38:05 NiMg-2FPy 1 PROP31DEC fgonzal + + + + + + +
9 19:06:59 RS-1-037_crude_C6D6_RT2hr_03232026 4 PROTON_SPIN_NoD_shim rshippy - + + - - + + hwcal: Width at half height : 8.13 Hz, Width at half height : 9.78 Hz, Width at half height : 10.51 Hz, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-037_crude_C6D6_RT2hr_03232026/4/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-037_crude_C6D6_RT2hr_03232026/4/pdata/1/peaks!
9 19:04:13 RS-1-037_crude_C6D6_RT2hr_03232026 3 P31CPD rshippy - + + - - + +
9 19:00:48 RS-1-037_crude_C6D6_RT2hr_03232026 2 P31CPD rshippy - + + - - + +
9 18:55:48 RS-1-037_crude_C6D6_RT2hr_03232026 1 PROTON_SPIN rshippy + + + + + + +
7 18:35:37 NiMg-NoEt2O 5 AAHSQC fgonzal - + + - - + +
7 18:10:33 NiMg-NoEt2O 4 C13CPD_SIENA fgonzal - + + - - + +
7 18:08:15 NiMg-NoEt2O 3 P31CPD fgonzal - + + - - + +
7 18:06:12 NiMg-NoEt2O 2 PROP31DEC fgonzal - + + - - + +
7 18:02:04 NiMg-NoEt2O 1 PROTON_SPIN fgonzal + + + + + + +
5 17:42:34 RS-1-037_crude_C6D6_10minstir_03232026 2 P31CPD rshippy - + + - - + +
5 17:37:18 RS-1-037_crude_C6D6_10minstir_03232026 1 PROTON_SPIN rshippy + + + + + + +
1 16:18:43 FG-1-194 8 P31CPD fgonzal - + + - - + +
1 16:14:25 FG-1-194 7 PROTON_SPIN fgonzal + + + + + + +
24 12:17:06 CW-05-142_13C 1 C13CPD_SIENA cwaller + + + + + + +
23 12:13:19 RS-1-034_crude_tol_150minRTstir_03232026 2 P31CPD rshippy - + + - - + +
23 12:08:30 RS-1-034_crude_tol_150minRTstir_03232026 1 PROTON_SPIN_NoD_shim rshippy + + + + - + + hwcal: Width at half height : 28.47 Hz; topshim: TopshimFieldMap - not enough valid points in centre: the gradient does not work, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-034_crude_tol_150minRTstir_03232026/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/rshippy/nmr/RS-1-034_crude_tol_150minRTstir_03232026/1/pdata/1/peaks!
22 11:47:35 KJ-2026-P-OMe_Nitrogen_2 3 AAHSQC kjacob - + + - - + +
22 10:13:27 KJ-2026-P-OMe_Nitrogen_2 2 C13CPD_POLYMER kjacob - + + - - + +
22 10:04:14 KJ-2026-P-OMe_Nitrogen_2 1 PROTON_SPIN kjacob + + + + + + +
22 10:03:24 KJ-2026-P-OMe_Nitrogen_2 1 PROTON_SPIN kjacob - - - - - - - Automation was stopped by user