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IconNMR Automation Run Status:
Day Experiments: 07:49
Busy Until: Fri 09:54
Night Experiments: 00:00

Setup List
Holder Status Name ExpNo Experiment User Time Title
44 Completed JG-01-267-A-4pm-01-15-2026 1 N PROTON_SPIN 1H experiment spin on jgipper 00:00:38
44 Completed JG-01-267-A-4pm-01-15-2026 2 N P31CPD 31P exp. comp. pulse decoupling jgipper 00:00:46
45 Completed JG-01-267-B-4pm-01-15-2026 1 N P31CPD 31P exp. comp. pulse decoupling jgipper 00:00:46
45 Completed JG-01-267-B-4pm-01-15-2026 2 N PROTON_SPIN 1H experiment spin on jgipper 00:00:38
47 Completed JG-01-267-A-4pm-01-15-2026 4 N DEUTERIUM 1D 2H jgipper 00:00:57
49 Completed CA-8 1 N PROTON_SPIN 1H experiment spin on sksingh 00:03:00 1D 1H temp=67C solvent=DMSO/TFA ns=32 d1=2s
49 Completed CA-8 2 N C13CPD_SIENA 1D 13C w/1H decoupling sksingh 00:22:30 1D 13C temp=67C solvent=DMSO/TFA ns=1k d1=0.15s
49 Running CA-8 3 N C13CPD_SIENA 1D 13C w/1H decoupling sksingh 13:09:22 1D q13C (quantitative) temp=67C solvent=DMSO/TFA ns=1k d1=45s
49 Submitted CA-8 4 N AACOSY 2D 1H-1H COSY sksingh 00:18:52 2D COSY temp=67C solvent=DMSO/TFA ns=2 d1=2s
49 Submitted CA-8 5 N AAHSQC echo/antiecho edited HSQC w/sensitivity improvement w/adiabatic bilevel decoupling w/adiabatic refocussing (w/ gradients in back-INEPT) sksingh 00:36:30 2D HSQC temp=67C solvent=DMSO/TFA ns=4 d1=2s
49 Submitted CA-8 6 N AAHMBC HMBCGPND sksingh 00:41:02 2D HMBC temp=67C solvent=DMSO/TFA ns=8 d1=2s
49 Submitted CA-8 7 N AATOCSYGP sksingh 01:17:30 2D TOCSY temp=67C solvent=DMSO/TFA ns=8 d1=2s
57 Completed BN2Bpin_T8hr 1 N PROTON_SPIN 1H experiment spin on kgour 00:00:24
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
49 17:47:38 CA-8 3 C13CPD_SIENA sksingh - + + - - - - 1D q13C (quantitative) temp=67C solvent=DMSO/TFA ns=1k d1=45s
49 17:22:41 CA-8 2 C13CPD_SIENA sksingh - + + - - + + 1D 13C temp=67C solvent=DMSO/TFA ns=1k d1=0.15s
49 17:18:27 CA-8 1 PROTON_SPIN sksingh - - + - - + + 1D 1H temp=67C solvent=DMSO/TFA ns=32 d1=2s
47 16:16:52 JG-01-267-A-4pm-01-15-2026 4 DEUTERIUM jgipper + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed, Automation was stopped by user
45 16:15:12 JG-01-267-B-4pm-01-15-2026 2 PROTON_SPIN jgipper - + + - - + + pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/jgipper/nmr/JG-01-267-B-4pm-01-15-2026/2/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/jgipper/nmr/JG-01-267-B-4pm-01-15-2026/2/pdata/1/peaks!
45 16:11:46 JG-01-267-B-4pm-01-15-2026 1 P31CPD jgipper + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
44 16:08:49 JG-01-267-A-4pm-01-15-2026 3 DEUTERIUM jgipper - + + - - + + sref: lock nucleus off not specified in /opt/topspin3.6.2/exp/stan/nmr/lists/nuclei.all SR is set to 0.0, sref: lock nucleus off not specified in /opt/topspin3.6.2/exp/stan/nmr/lists/nuclei.all SR is set to 0.0
44 16:05:11 JG-01-267-A-4pm-01-15-2026 2 P31CPD jgipper - + + - - + +
44 16:01:06 JG-01-267-A-4pm-01-15-2026 1 PROTON_SPIN jgipper + + + + + + +
57 14:26:42 BN2Bpin_T8hr 1 PROTON_SPIN kgour + + + + + + +
55 14:01:15 VF_2_420E_3h 1 PROTON_SPIN vfadare + + + + + + +
54 13:56:07 VF_2_420E_2h 1 PROTON_SPIN vfadare + + + + + + +
53 13:51:41 VF_2_420E_1h w std 1 PROTON_SPIN vfadare + + + + + + +
53 13:19:45 VF_2_420E_1h_w.o std 1 PROTON_SPIN vfadare + + + + + + +
52 13:10:35 0113SBNI30-35 1 PROTON_SPIN khuang + + + + + + +
51 13:04:21 0113SBNI25-29 1 PROTON_SPIN khuang + + + + + + +
50 12:58:08 0113SBNI24-25 1 PROTON_SPIN khuang + + + + + + +
49 12:52:00 0113SBNI22-24 1 PROTON_SPIN khuang + + + + + + +
48 12:45:22 0113SBNI20-21 1 PROTON_SPIN khuang + + + + + + +
47 12:33:31 VF_2_417C_slt_me 1 PROTON_SPIN vfadare + + + + + + +
45 12:06:42 JR-1-179 b PA control 3 C13CPD_SIENA jrana - + + - - + +
45 12:01:05 JR-1-179 b PA control 2 PROTON_SPIN jrana + + + + + + +
44 11:56:56 JG-01-269-1155am-01-15-2026 2 P31CPD jgipper - + + - - + +
44 11:53:59 JG-01-269-1155am-01-15-2026 1 PROTON_SPIN jgipper + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/jgipper/nmr/JG-01-269-1155am-01-15-2026/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/jgipper/nmr/JG-01-269-1155am-01-15-2026/1/pdata/1/peaks!
41 09:34:04 CW-05-042_13C 2 C13CPD_SIENA cwaller + + + + + + +
41 09:24:45 CW-05-042_13C 1 PROTON_SPIN cwaller + + + + + + +
39 03:17:05 NL-UO2H3-20260114 1 PROTON_SPIN nlind + + + + + + +
38 03:11:46 to-51-5-1 1 PROTON_SPIN tojanov + + + + + + +
28 03:08:16 AE-TBP-31P 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
27 03:04:46 AE-U2-TBP-31P 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
26 03:01:01 AE-TOPO-31P 2 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
25 02:56:57 AE-U2-TOPO-31P 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
40 02:00:55 MN1-96-C-COLUMN-F12 3 AAHSQC nmahesh - + + - - + x pp: Unable to assign a peak for scaling of /opt/topspin/data/nmahesh/nmr/MN1-96-C-COLUMN-F12/3/pdata/1000/peaks No peak is found in the specified ranges!, pp: Unable to assign a peak for scaling of /opt/topspin/data/nmahesh/nmr/MN1-96-C-COLUMN-F12/3/pdata/1000/peaks No peak is found in the specified ranges!
40 23:04:49 MN1-96-C-COLUMN-F12 2 C13DEPT135_SIENA nmahesh - + + - - + +
40 23:00:00 MN1-96-C-COLUMN-F12 1 PROTON_SPIN nmahesh + + + + + + +
37 22:53:47 TO-51-3-1 1 PROTON_SPIN tojanov + + + + + + +
36 22:43:08 DZ-0071-070 3 C13CPD_SIENA jgalvez - + + - - + +
36 22:34:50 DZ-0071-070 2 AACOSY jgalvez - + + - - + +
36 22:29:31 DZ-0071-070 1 PROTON_SPIN jgalvez + + + + + + +
35 22:18:51 DZ-0070-105-A 3 C13CPD_SIENA tzehnder - + + - - + +
35 22:10:33 DZ-0070-105-A 2 AACOSY tzehnder - + + - - + +
35 22:05:28 DZ-0070-105-A 1 PROTON_SPIN tzehnder + + + + + + +
34 22:00:10 DZ-0070-105-B 1 PROTON_SPIN tzehnder + + + + + + +
33 20:28:15 JR-1-179 pH 12.34 3 AAHSQC jrana - + + - - + +
33 18:37:21 JR-1-179 pH 12.34 2 C13CPD_SIENA jrana - + + - - + +
33 18:31:39 JR-1-179 pH 12.34 1 PROTON_SPIN jrana + + + + + + +
32 18:26:35 DZ-0070-103-D-f33 1 PROTON_SPIN tzehnder + + + + + + +
31 18:21:16 DZ-0070-103-C-f34 1 PROTON_SPIN tzehnder + + + + + + +
30 18:15:59 DZ-0070-103-E-f27 1 PROTON_SPIN tzehnder + + + + + + +
29 17:49:17 CW-05-041_13C 1 C13CPD_SIENA cwaller + + + + + + +
28 17:45:48 AE-TBP-20260114 1 PROTON_SPIN aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/aervin/nmr/AE-TBP-20260114/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/aervin/nmr/AE-TBP-20260114/1/pdata/1/peaks!
27 17:42:09 AE-U2-TBP-20260114 1 PROTON_SPIN aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/aervin/nmr/AE-U2-TBP-20260114/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/aervin/nmr/AE-U2-TBP-20260114/1/pdata/1/peaks!
26 17:38:44 AE-TOPO-20260114 1 PROTON_SPIN aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/aervin/nmr/AE-TOPO-20260114/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/aervin/nmr/AE-TOPO-20260114/1/pdata/1/peaks!
25 17:34:57 AE-U2-TOPO-20260114 1 PROTON_SPIN aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/aervin/nmr/AE-U2-TOPO-20260114/1/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/aervin/nmr/AE-U2-TOPO-20260114/1/pdata/1/peaks!
45 16:47:56 JR-1-179 3 AAHSQC jrana - + + - - + +
45 16:23:37 JR-1-179 2 C13CPD_SIENA jrana - + + - - + +
45 16:19:03 JR-1-179 1 PROTON_SPIN jrana + + + + + + +
43 12:31:00 BN2BPin_T3hr_Re 1 PROTON_SPIN kgour + + + + + + +
42 12:26:58 KG_117_T6hr 1 PROTON_SPIN kgour + + + + + + +
39 10:43:24 FC-37-box 1 PROTON_SPIN fcooper + + + + + + +
36 10:17:06 KG_117_T4hr 1 PROTON_SPIN kgour + + + + + + +
35 10:12:46 4-MB1S_T4hr 1 PROTON_SPIN kgour + + + + + + +
52 09:28:16 JG-01-268-B 2 PROTON_SPIN jgipper - + + - - + +
52 09:24:41 JG-01-268-B 1 P31CPD jgipper + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
52 09:21:00 JG-01-268-B 1 P31CPD jgipper + + + x - - - Lock failed after multiple attempts, lock: No status change after 'LOCK on'. -> aborted!, No status change after 'LOCK on'. -> aborted!
51 09:17:23 JG-01-268-A 2 P31CPD jgipper - + + - - + +
51 09:11:37 JG-01-268-A 1 PROTON_SPIN jgipper + + + + x + + topshim: TopshimSetShims - BSMS limits exceeded, Shim failed
49 08:53:21 BN2BPin_T3hr 1 PROTON_SPIN kgour + + + + + + +
48 08:49:38 KG_117_T3hr 1 PROTON_SPIN kgour + + + + + + +
47 08:45:57 KG_Silane_98 1 PROTON_SPIN kgour + + + + + + +
46 08:42:19 KG_Silane_P 1 PROTON_SPIN kgour + + + + + + +
45 08:38:41 KG_Silane_E 1 PROTON_SPIN kgour + + + + + + +
44 08:35:23 4-MB1S_T3hr 1 PROTON_SPIN kgour + + + + + + +
39 07:59:37 4-MB1S_T2.5hr 1 PROTON_SPIN kgour + + + + + + +
36 07:55:44 KG_117_T2hr 1 PROTON_SPIN kgour + + + + + + +
36 06:32:46 KG_117_T1hr 1 PROTON_SPIN kgour + + + + + + +
35 06:28:47 BN2BPin_T1hr 1 PROTON_SPIN kgour + + + + + + +
34 06:25:10 4-MB1S_T1hr 1 PROTON_SPIN kgour + + + + + + +
33 06:21:36 4-MB1B_T1hr 1 PROTON_SPIN kgour + + + + + + +
29 05:17:10 KG_117_T0 1 PROTON_SPIN kgour + + + + + + +
28 05:12:44 BN2Bpin_T0 1 PROTON_SPIN kgour + + + + + + +
27 05:09:05 4-MB1S_T0 1 PROTON_SPIN kgour + + + + + + +
26 05:04:59 4-MB2B_T0 1 PROTON_SPIN kgour + + + + + + +
46 19:28:11 AB-01-520-P 2 C13CPD_SIENA ajiskani - + + - - + +
46 19:23:17 AB-01-520-P 1 PROTON_SPIN ajiskani + + + + + + +
45 19:18:33 DZ-0070-104-B 1 PROTON_SPIN tzehnder + + + + + + +
44 19:13:32 DZ-0070-104-A 1 PROTON_SPIN tzehnder + + + + + + +
43 19:07:54 DZ-0070-100-A 1 PROTON_SPIN tzehnder + + + + + + +
42 18:57:12 DZ-0070-103-B 3 C13CPD_SIENA tzehnder - + + - - + +
42 18:48:53 DZ-0070-103-B 2 AACOSY tzehnder - + + - - + +
42 18:43:43 DZ-0070-103-B 1 PROTON_SPIN tzehnder + + + + + + +
41 18:33:03 DZ-0070-103-A 3 C13CPD_SIENA tzehnder - + + - - + +
41 18:24:42 DZ-0070-103-A 2 AACOSY tzehnder - + + - - + +
41 18:19:30 DZ-0070-103-A 1 PROTON_SPIN tzehnder + + + + + + +
40 17:55:39 AB-01-519-P 2 C13CPD_SIENA ajiskani - + + - - + +
40 17:50:59 AB-01-519-P 1 PROTON_SPIN ajiskani + + + + + + +
39 17:39:05 DZ-0066-133-A 3 C13CPD_SIENA tzehnder - + + - - + +
39 17:30:42 DZ-0066-133-A 2 AACOSY tzehnder - + + - - + +
39 17:25:06 DZ-0066-133-A 1 PROTON_SPIN tzehnder + + + + + + +
38 17:22:50 FG-1-161-Out-Green 2 P31CPD fgonzal - + + - - + +
38 17:18:56 FG-1-161-Out-Green 1 PROTON_SPIN fgonzal + + + + + + +
37 17:17:20 FG-1-161-Out-Brown 2 PROTON_SPIN fgonzal - + + - - + +
37 17:11:43 FG-1-161-Out-Brown 1 P31CPD fgonzal + + + + + + +
36 17:07:31 FG-1-161-In-Brown 2 P31CPD fgonzal - + + - - + +
36 17:03:16 FG-1-161-In-Brown 1 PROTON_SPIN fgonzal + + + + + + +
35 16:58:25 GZ01_268_band3 1 PROTON_SPIN gzhang + + + + + + +
34 16:56:05 PAT_2025_039_New 5 PROTON_SPIN padelow - + + - - + +
34 16:34:53 PAT_2025_039_New 4 AAHSQC padelow - + + - - + +
34 15:25:33 PAT_2025_039_New 3 C13CPD_SIENA padelow - + + - - + +
34 15:23:47 PAT_2025_039_New 2 PROTON_SPIN padelow - - + - - + +
34 15:09:24 PAT_2025_039_New 1 PROTON_SPIN padelow + + + + + + + Automation was stopped by user
32 14:05:45 024_DMSO 3 AAHSQC padelow - + + - - + +
32 13:18:20 024_DMSO 2 C13CPD_SIENA padelow - + + - - + +
32 13:13:33 024_DMSO 1 PROTON_SPIN padelow + + + + + + +
31 13:09:59 AE-2-184-7 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
30 13:06:37 AE-2-184-6 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
29 13:03:12 AE-2-184-5 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
28 12:59:39 AE-2-184-4 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
27 12:56:14 AE-2-184-3 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
26 12:52:14 AE-2-184-2 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
25 12:46:23 AE-2-184-1 1 P31CPD aervin + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
46 11:47:38 PAT_2025_024_NEW 3 AAHSQC padelow - + + - - + +
46 11:12:34 PAT_2025_024_NEW 2 C13CPD_SIENA padelow - + + - - + +
46 11:07:12 PAT_2025_024_NEW 1 PROTON_SPIN padelow + + + + + + +
45 10:47:56 PAT_2025_013_NEW 3 AAHSQC padelow - - + - - + +
45 10:17:13 PAT_2025_013_NEW 2 C13CPD_SIENA padelow - + + - - + + log_err: Error in ipsoControl::checkStatus(): Status line active! Error in Master: Error 220 in SGU1: -- SLOT 4 RACK 1: AQS1 Board Timeout Error 112 in SGU1: -- SLOT 4 RACK 1: SGU1 AE SLOT 4 RACK 1: SBSB Wake-Up occured during acquisition, SGU CPU reboot Error 6 in SGU1: -- SLOT 4 RACK 1: Too many slave errors, slave access impossible Error 220 in SGU2: -- SLOT 5 RACK 1: AQS1 Board Timeout Error 220 in RX_1: -- SLOT 2 RACK 1: AQS1 Board Timeout, Automation was stopped by user
45 10:15:06 PAT_2025_013_NEW 1 PROTON_SPIN padelow - - + - - + +
45 10:05:37 PAT_2025_013_NEW 1 PROTON_SPIN padelow + + + x - - - Lock failed after multiple attempts, lock: Command 'lock CDCl3' failed. Lock is OFF, Command 'lock CDCl3' failed. Lock is OFF, Automation was stopped by user
43 09:27:06 JG-01-266-915am-01-13-2026 2 P31CPD jgipper - + + - - + +
43 09:16:22 JG-01-266-915am-01-13-2026 1 PROTON_SPIN jgipper + + + + + + +
40 19:10:28 NL-UO2LBnt3-para-20260112 1 PROTON_SPIN nlind + + + + + + +
36 18:38:32 NL-UO2Bnt3-20260112 1 PROTON_SPIN nlind + + + + + + +
34 18:13:28 Ab-01-518-PURE 2 C13CPD_SIENA ajiskani - + + - - + +
34 18:07:41 Ab-01-518-PURE 1 PROTON_SPIN ajiskani + + + + + + +
29 17:45:06 TO-META-number 1 PROTON_SPIN tojanov + + + + + + +
27 17:42:58 JG-01-266-530pm-01-12-2026-1h-8scan 8 P31CPD jgipper - + + - - + +
27 17:41:09 JG-01-266-530pm-01-12-2026-1h-8scan 7 P31CPD jgipper - + + - - + +
27 17:37:59 JG-01-266-530pm-01-12-2026-1h-1scan 9 P31CPD jgipper - + + - - + +
27 17:36:54 JG-01-266-530pm-01-12-2026-1h-1scan 4 PROTON_SPIN jgipper - + + - - + +
27 17:35:21 JG-01-266-530pm-01-12-2026-1h-16scan 3 PROTON_SPIN jgipper - + + - - + +
27 17:31:18 JG-01-266-530pm-01-12-2026-1h-8scan 1 PROTON_SPIN jgipper + + + + + + +
48 16:36:49 KG_4methylbenzaldehyde 1 PROTON_SPIN kgour + + + + + + +
45 16:16:39 KJ_aminemore 4 AAHSQC kjacob - + + - - + +
45 16:01:37 KJ_aminemore 3 C13DEPT135_SIENA kjacob - + + - - + +
45 15:37:19 KJ_aminemore 2 C13CPD_SIENA kjacob - + + - - + +
45 15:31:40 KJ_aminemore 1 PROTON_SPIN kjacob + + + + + + +
41 15:11:34 KJ_amineless 4 AAHSQC kjacob - + + - - + +
41 14:56:34 KJ_amineless 3 C13DEPT135_SIENA kjacob - + + - - + +
41 14:32:33 KJ_amineless 2 C13CPD_SIENA kjacob - + + - - + +
41 14:27:44 KJ_amineless 1 PROTON_SPIN kjacob + + + + + + +
37 14:07:34 PAT_2026_093 3 AAHSQC padelow - + + - - + +
37 13:31:18 PAT_2026_093 2 C13CPD_SIENA padelow - + + - - + +
37 13:25:46 PAT_2026_093 1 PROTON_SPIN padelow + + + + + + +
35 12:51:20 JG-01-265-1245PM-01-12-2026 2 PROTON_SPIN jgipper - + + - - + + pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/jgipper/nmr/JG-01-265-1245PM-01-12-2026/2/pdata/1/peaks!, pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of /opt/topspin/data/jgipper/nmr/JG-01-265-1245PM-01-12-2026/2/pdata/1/peaks!
35 12:46:15 JG-01-265-1245PM-01-12-2026 1 P31CPD jgipper + + + + x + + topshim: TopshimCheckLockAndSample - lock is off: please lock in prior to shimming, Shim failed
33 12:05:58 JR-1-178 pH 12.34 4 P31 jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'DMSO' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'DMSO' SR is set to 0.0
33 11:23:49 JR-1-178 pH 12.34 3 P31HSQC jrana - + + - - + +
33 11:20:06 JR-1-178 pH 12.34 2 P31CPD jrana - + + - - + + sref: NUCLEUS '31P' not defined for SOLVENT 'DMSO' SR is set to 0.0, sref: NUCLEUS '31P' not defined for SOLVENT 'DMSO' SR is set to 0.0
33 11:14:29 JR-1-178 pH 12.34 1 PROTON_SPIN jrana + + + + + + +